Publications

Short SiC fiber/Ti3SiC2 MAX phase composites: Fabrication and creep evaluation

Dash, A. and Malzbender, J. and Vaßen, R. and Guillon, O. and Gonzalez-Julian, J.

JOURNAL OF THE AMERICAN CERAMIC SOCIETY
Volume: 103 Pages: 7072-7081
DOI: 10.1111/jace.17337
Published: 2020

Abstract
The compressive creep of silicon carbide fiber reinforced Ti3SiC2 MAX phase with both fine and coarse microstructure was investigated in the temperature range of 1000-1300°C. Comparison of only steady-state creep was done to understand the response of fabricated composite materials toward creep deformation. It was demonstrated that the fibers are more effective in reducing the creep rates for the coarse microstructure by an increase in activation energy compared to the variant with a finer microstructure, being partly a result of the enhanced creep rates for the microstructure with larger grain size. Grain boundary sliding along with fiber fracture appears to be the main creep mechanism for most of the tested temperature range. However, there are indications for a changed creep mechanism for the fine microstructure for the lowest testing temperature. Local pores are formed to accommodate differences in strain related to creeping matrix and predominantly elastically deformed fibers during creep. Microstructural analysis was done on the material before and after creep to understand the deformation mechanics. © 2020 The Authors. Journal of the American Ceramic Society published by Wiley Periodicals LLC on behalf of American Ceramic Society (ACERS)

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